Fertile formulations

Having established in-house coating and testing of solid fertiliser, a Nynas researcher finds that naphthenic process oils offer coating formulations capable of reducing both dust and caking issues.

Emma Öberg

Development Engineer
Nynas AB

Being hygroscopic, solid fertiliser tends to absorb moisture, leading to caking and handling issues. The fertiliser can also create dust, a work environment hazard. However, both these issues can be addressed by coating the fertiliser, and process oil can be used either neat or in formulated coatings, also containing wax and hydrophobic amines.

Unfortunately, there are only a few standard methods for coating fertiliser or for relevant testing of coated solid fertiliser on a lab scale, so in order to study how their naphthenic process oil products perform in this application, Nynas had to develop their own in-house coating and testing equipment and procedures.

“Fertiliser producers or their coating formulators often use their own internal methods, but we wanted to be able to prepare and test fertiliser coatings in our own lab,” explains Emma Öberg, Development Engineer at Nynas.

Having set up a testbed for the comparative evaluation of different oils, she was able to determine that naphthenic process oils offer benefits and can be used to replace diminishing volumes of Group I oils in this application. However, Nynas products also showed performance advantages compared with Group II oils.

“The study shows that naphthenic process oils keep amines in solution at lower temperatures than Group I or Group II oils. This allows an anti- caking coating to be sprayed at lower temperatures, enabling cost reductions for processors,” says Emma Öberg.

Amine and oil blends prepared with the naphthenic mineral oil NYTEX® 820 had a lower cloud point compared with Group I and Group II oils of the same viscosity, indicating higher solvent power. Figure 1. shows the correlation between the cloud point for amine and oil blends and the respective oil’s aniline point.

The study also looked at the anti-dust performance of various Nynas products. Figure 2. shows the dusting tendency of untreated and oil coated multi-nutrient NPK (Nitrogen, Phosphorous and Potassium) fertiliser. The results indicate that dust levels can be significantly reduced by coating the fertiliser with a naphthenic process oil.

“Testing different oils showed that the addition of Nynas process oil to NPK fertiliser reduced dust by 50 percent,” says Emma Öberg.

Coatings Checklist

The results of Nynas’ fertiliser coatings study can be summarised in a checklist for coatings formulators or fertiliser companies.

  • Naphthenic process oils have higher solvency and will keep amines in solution at lower temperatures than Group I and Group II oils.
  • A higher nitrogen content will typically make the fertiliser cake more easily.
  • Consider the fertiliser’s Critical Relative Humidity (CRH) value when estimating which type of coating is needed.
  • Choose oils of low colour to coat Calcium Ammonium Nitrate (CAN) if it is important to keep its white colour intact.
  • Ammonium sulfate (AS) has lower caking tendency, so will need mainly anti-dust coating.

Figure 1. Correlation between cloud point for amine and oil blends and aniline point of the oil. Oil aniline point: Group I (115 cSt at 40 °C, AP 116°C), Group II (106 cSt at 40 °C, AP 126°C), NYTEX® 820 (110 cSt at 40 °C, AP 86°C).

Figure 2. The dusting tendency of NPK fertiliser can be significantly reduced by coating with a naphthenic process oil.

Further reading

Solvency offers great solutions

High solvent power is the secret of the success of naphthenic oils in chemical applications. Anna Eriksson, Technical Manager, Nynas Naphthenics, offers a couple of examples that explain why.

Perfecting purification

In a study aimed at finding the most effective purifying oil for crude titanium tetrachloride, Nynas’ researchers obtained near perfection from one mineral oil and promising results from a hybrid biogenic oil.

Hot solution for hot melts

By boosting the compatibility of ingredients, naphthenic mineral oils are providing hot melt adhesive manufacturers with new and more flexible formulations

THERE IS MORE TO US THAN THIS

We are delighted you are interested in our products. If you have any questions about our products and services, get in touch with your local Nynas contact. Besides top quality oils, we offer a wide range of services, including rapid delivery worldwide, training, seminars and much more. All you have to do is ask.

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Marcela Tocelis

Sales Manager / Acting General Manager

 Martin Vergara

Martin Vergara

Customer Service Executive

 Juan Pablo Pace

Juan Pablo Pace

Customer Service Coordinator

Eric Alfosea

Eric Alfosea

Sales Manager France

 Stéphanie Ly

Stéphanie Ly

Customer Service Executive

 Christine Le Garrec

Christine Le Garrec

Customer Service Coordinator

Sheilo Mienandi

Sheilo Mienandi

Customer Service Coordinator

Emil Cuculayef

Emil Cuculayef

Sales Manager

 Banu Kibar

Banu Kibar

Customer Service Executive

Cagatay Gürol

Customer Service Coordinator

David Barnett

David Barnett

General Manager

 Samantha Moodley

Samantha Moodley

Customer Service Executive

Lee Anne Williams

Lee Anne Williams

Customer Service Coordinator

 Sameen Kadli

Sameen Kadli

Sales Manager

Shoeb Ahmed

Shoeb Ahmed

Customer Service Coordinator

 Sibala Libish Kumar

Sibala Libish Kumar

Global Customer Service Specialist & Project lead

 Marcela Tocelis

Marcela Tocelis

Sales Manager / Acting General Manager

 Martin Vergara

Martin Vergara

Customer Service Executive

 Juan Pablo Pace

Juan Pablo Pace

Customer Service Coordinator

 Marcela Tocelis

Marcela Tocelis

Sales Manager / Acting General Manager

 Marcela Tocelis

Marcela Tocelis

Sales Manager / Acting General Manager

 Martin Vergara

Martin Vergara

Customer Service Executive

 Juan Pablo Pace

Juan Pablo Pace

Customer Service Coordinator

Lawrence Teo

Lawrence Teo

Area Sales Manager

 Georgina Ng

Georgina Ng

Customer Service Executive

Alistair Meyer

Alistair Meyer

Regional Director

David Barnett

David Barnett

General Manager

 Samantha Moodley

Samantha Moodley

Customer Service Executive

Lee Anne Williams

Lee Anne Williams

Customer Service Coordinator

David Barnett

David Barnett

General Manager

 Samantha Moodley

Samantha Moodley

Customer Service Executive

Lee Anne Williams

Lee Anne Williams

Customer Service Coordinator